HEPL

For the lecture: general chemistry of bachelor. For the laboratory work: safety requirements, know-how acquired at the general chemistry laboratory

To acquire the principles of various methods in quantitative chemical analysis (traditional techniques, electrochemical methods or chromatographic methods, in mineral, organic or biochemical fields) in front of a particular analytical problem, to reach the capacity to select the appropriate working method to its resolution. To acquire, by handling of laboratory, the rigour of work necessary to obtain right and precise analytical results as well as a know-how in traditional and electrochemical analyses.

Traditional methods (lecture): errors; techniques of sampling, put in solution,; gravimetry, precipitation; titrimetry (by precipitation, neutralization, oxydoreduction, complexation); gazometry; separations via precipitation, complexation, liquid-liquid extraction ; acidimetry in nonaqueous medium. Electrochemical methods (lecture): conductimetry, potentiometry , electrogravimetry, coulometry, polarography, amperometry. Separative methods (lecture): gas chromatography, column, thin layer, HPLC, methods by external, internal calibration and proportioned addition; electrophoresis. Laboratory work: gravimetry; titrimetry (acid-base, oxydoreduction, precipitation, complexation) ; gazometry; distillation ; conductimetry; electrogravimetry; potentiometry; coulometry, Karl Fisher.

Fiefield W., Kealey D., Principles and practice of analytical chemistry Blackie, 1990

Rouessac F., Rouessac A., Analyse chimique, Méthodes et techniques instrumentales modernes, Masson, 1995